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005 20231106095349.0
008 231030b ||||| |||| 00| 0 eng d
022 _a0021-9584
037 _bRIEBPL Library
082 _a540.7
100 _aLauren I. Austen et al ...
245 _aByproduct Valorization: From Spent Coffee Grounds to Fatty Acid Ethyl Esters
_b(Journal Article)
_c
260 _aWashington, United States
_b:American Chemical Society
_c,January 10, 2023
300 _a327-335p.
490 _aAmerican Chemical Society, Volume 100, Issue 1
505 _a***______{For Hard Copy, Please visit Library.}________***
520 _aAbstract:- A laboratory experiment was designed to provide students with an introduction to byproduct valorization by producing an analogue of biodiesel (fatty acid ethyl esters, FAEE) via lipid extraction and subsequent transesterification from spent coffee grounds (SCG). Valorization is the process of upgrading underutilized or discarded wastes or byproducts into chemicals, materials, and (bio)energy. Upon isolation of the intermediate and FAEE, students analyzed the respective spectroscopic characteristics using infrared and nuclear magnetic resonance spectroscopy as well as evaluated gas chromatography spectra that were provided. Associated green metrics for the reaction were determined to obtain a quantitative measure of the “greenness” of the experiment. In this laboratory experiment, students are introduced to key concepts such as whole systems thinking and the United Nations Sustainable Development Goals where they apply these frameworks to real-world problems such as consumption and waste disposal. In addition to providing a greener alternative to traditional methods for biodiesel analogue production from SCG by solvent alterations, this experiment demonstrates the value of waste that would otherwise be overlooked to generate products that can help reduce the continued use of finite fossil fuels.
650 _aGreen Chemistry Second-Year
650 _aUndergraduate Analytical
650 _aChemistry Laboratory Instruction
650 _aHands-on Learning/Manipulatives
650 _aFatty Acids Lipids
856 _uhttps://pubs.acs.org/doi/epdf/10.1021/acs.jchemed.2c00728
942 _cPER
999 _c44689
_d44688