Toward Qualified Synthetic Chemist. Step 1 (Record no. 45261)
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| 000 -LEADER | |
|---|---|
| fixed length control field | 02337nam a22002057a 4500 |
| 005 - DATE AND TIME OF LATEST TRANSACTION | |
| control field | 20240116143254.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 240116b ||||| |||| 00| 0 eng d |
| 022 ## - INTERNATIONAL STANDARD SERIAL NUMBER | |
| ISSN | 0021-9584 |
| 100 ## - MAIN ENTRY--AUTHOR NAME | |
| Personal name | Volochnyuk, Dmitriy M. |
| 245 ## - TITLE STATEMENT | |
| Title | Toward Qualified Synthetic Chemist. Step 1 |
| Remainder of title | : Building and Assessing Basic Skills in Organic Synthesis (Journal Article) |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. (IMPRINT) | |
| Place of publication | Washington DC |
| Name of publisher | : American Chemical Society |
| Year of publication | , 2023 |
| 300 ## - PHYSICAL DESCRIPTION | |
| Number of Pages | 3309–3319p. |
| 440 ## - SERIES STATEMENT/ADDED ENTRY--TITLE | |
| Title | Journal of Chemical Society |
| Volume number/sequential designation | , Volume 100: Number 9, September 2023 |
| 505 ## - FORMATTED CONTENTS NOTE | |
| Formatted contents note | ***______{For Hard Copy, Please visit Library.}________***<br/><br/> |
| 520 ## - SUMMARY, ETC. | |
| Summary, etc | Abstract: An introductory experimental course to teach and assess basic organic synthesis and identification skills has been designed. The first work of this course, which is based on the well-known hydrazone formation reaction of benzaldehydes with Brady’s reagent, is presented. The designed experiment has many advantages and perfectly matches the goal of teaching rookie chemists. At the same time, the work allows one to fasten such primary laboratory skills as a measurement of the mass of a solid substance; measurement of the volume of a liquid; the use of a laboratory apparatus for filtration under reduced pressure; making calculations of yield neatness and accuracy in doing the work; the ability of students to make and record qualitative observations. Apart from teaching, the work emphasizes the quantitative assessment of students’ skills and the development of a clear and easy-to-use grading scale including all basic quality parameters of a reaction product. Additionally, a comprehensive analysis of how students’ mistakes contribute to the products’ yield and purity as well as the time required for the accomplishment of the experiment was performed. The proper design of the experiment and precise quality control of the product help to answer the question, “What have the students done wrong while performing the work?”. |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical Term | High School/Introductory Chemistry| First-Year Undergraduate| General/Organic Chemistry| Assessment| Synthesis| Identification |
| 700 ## - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Makhankova, Valeriya G. | Lyapunov, Alexander Yu. | Muravska, Liliia S. | Vitsenko, Olexander M. | Ryabukhin, Sergey V. |
| 856 ## - ELECTRONIC LOCATION AND ACCESS | |
| Uniform Resource Identifier | https://doi.org/10.1021/acs.jchemed.2c01214 |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Koha item type | Periodicals |
| Lost status | Damaged status | Home library | Current library | Date acquired | Koha item type |
|---|---|---|---|---|---|
| RIE BPL Library | RIE BPL Library | 16.01.2024 | Periodicals |