MARC details
| 000 -LEADER |
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| fixed length control field |
02406nam a22003137a 4500 |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20231103145016.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
231030b ||||| |||| 00| 0 eng d |
| 022 ## - INTERNATIONAL STANDARD SERIAL NUMBER |
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| ISSN |
0021-9584 |
| 037 ## - SOURCE OF ACQUISITION |
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| Source of stock number/acquisition |
RIEBPL Library |
| 082 ## - DEWEY DECIMAL CLASSIFICATION NUMBER |
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| Classification number |
540.7 |
| 100 ## - MAIN ENTRY--AUTHOR NAME |
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| Personal name |
Alain M. Beauparlant et al... |
| 245 ## - TITLE STATEMENT |
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| Title |
Teaching Single Crystal X-ray Crystallography in the Undergraduate Classroom with Sugar and Epsom Salt |
| Remainder of title |
(Journal Article) |
| Statement of responsibility, etc |
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| 260 ## - PUBLICATION, DISTRIBUTION, ETC. (IMPRINT) |
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| Place of publication |
Washington, United States |
| Name of publisher |
:American Chemical Society |
| Year of publication |
,January 10, 2023 |
| 300 ## - PHYSICAL DESCRIPTION |
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| Number of Pages |
336-341p. |
| 490 ## - SERIES STATEMENT |
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| Series statement |
American Chemical Society, Volume 100, Issue 1 |
| 505 ## - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
***______{For Hard Copy, Please visit Library.}________*** |
| 520 ## - SUMMARY, ETC. |
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| Summary, etc |
Abstract-<br/><br/> We developed a single crystal X-ray crystallography experiment based on the crystal structure of sucrose (table sugar), and a more challenging experiment using Epsom salt. Both crystals are readily available in X-ray quality crystalline form. In these experiments, students mounted a crystal on a MiTeGen loop and analyzed it using a Rigaku XtaLAB Mini diffractometer (built 2011). Students generated models of both compounds using CrysAlisPro, Olex2, SHELXT, and SHELXL. All aspects of this experiment use free software programs which have user-friendly interfaces. A step-by-step laboratory protocol for determining the structure of both compounds is included in the Supporting Information. These experiments were used in the Fall of 2019 at the Junior and the Senior level. In the Summer of 2020, a take-home version of the lab was created in response to the Novel 2019 Coronavirus (COVID-19) pandemic and implemented in the General Chemistry laboratory curriculum; this experiment was used for the duration of the 2020–2021 academic year. These experiments are suitable for all undergraduate experience levels.<br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/><br/> |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical Term |
First-Year Undergraduate/General |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical Term |
Second-Year Undergraduate |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical Term |
Upper-Division Undergraduate |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical Term |
Laboratory Instruction Hands-On Learning/Manipulatives |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical Term |
Crystals/Crystallography Laboratory |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical Term |
Equipment/Apparatus |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical Term |
Inquiry-Based/Discovery |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical Term |
Learning Problem Solving/Decision |
| 650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical Term |
Making X-ray Crystallography |
| 856 ## - ELECTRONIC LOCATION AND ACCESS |
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| Uniform Resource Identifier |
https://doi.org/10.1021/acs.jchemed.2c00795 |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) |
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| Koha item type |
Periodicals |
